Tetrahedron

Isolation and synthesis of 3-chlorogentisyl alcohol—a metabolite of penicillium canadense

NJ McCorkindale, TP Roy, SA Hutchinson

Index: McCorkindale,N.J. et al. Tetrahedron, 1972 , vol. 28, p. 1107 - 1111

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Citation Number: 14

Abstract

... EXPERIMENTAL R,s refer to 0.25 mm layen of Kiesclgcl G. using p-aminoazobenum and Sudan yellow as standards ... Page 4. 1110 NJ MCCORKINDALE. TP ROY and SA H~J~CHIF~ON ... mp 147'. R,0.24(4?< McOH in CHCI,), v,,(KBr)cm-': 3374 A,, (ErOH), 283 (c 2370): J._(EtOH-NaOH) 303 (3840) NMR spectrum as in Table, mass spectrum m/e (relative abundance) 176 (33), 174 (loo), I59 (S), 158(7). 157(18), 156(18), lSS(ll), l47(9), 145(28). l39(73). 137(18). ...