Synthesis of 14C??labelled nitrosamines. IV synthesis of 14C??methyl??(1??acetoxy) methyl nitrosamine and 1??14C??ethyl (acetoxy) ethyl nitrosamine

H Braun, M Wiessler

Index: Braun; Wiessler Journal of Labelled Compounds and Radiopharmaceuticals, 1978 , vol. 14, # 6 p. 887 - 892

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Citation Number: 5

Abstract

Abstract A scheme is developed for synthesizing 14 C labelled α-acetates of secondary α- hydroxylated nitrosamines. In this manner 14 C-methyl (1-acetoxy) ethyl nitrosamine and 1- 14 C-ethyl (1-acetoxy) ethyl nitrosamine are synthesized in 16.3 and 33.3% yield, radiochemically pure.