Tetrahedron letters

Facile synthesis of azides: Conversion of hydrazines using dinitrogen tetroxide

YH Kim, K Kim, SB Shim

Index: Kim, Yong Hae; Kim, Kweon; Shim, Sung Bo Tetrahedron Letters, 1986 , vol. 27, # 39 p. 4749 - 4752

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Citation Number: 25

Abstract

Download full text in PDF Opens in a new window. Article suggestions will be shown in a dialog on return to ScienceDirect. ... Please enable JavaScript to use all the features on this page. ... Various hydrazines such as aryl-, carbonyl-, and sulfonyl-hydrazine were reacted with dinitrogen tetroxide to give the corresponding azides in excellent yields under mild conditions at low temperature(−20~− 40 °C) in acetonitrile. ... N 2 O 4 is commerially available or can be ...

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