Organic Preparations and Procedures International

An improved synthesis of 3-cyano-4-fluorobenzyl bromide

GA Cain

Index: Organic Preparations and Procedures International, , vol. 32, # 1 p. 88 - 91

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Abstract

... 12. L. Stefaniak, GA Webb and M. Witanowski, ibid., Vol. 18, p. 72 (1986). ... The literature synthesis6 reports a two-step preparation. Our in-house synthesis of this starting material proceeded in 80% yield. ... The organic phase was dried (Na,SO,), filtered, and concentrated in uucuo. ...