A New Route to 1, 3-Dienes: TMSI Elimination of 2-Ene-1, 4-diols

RK Hill, SL Pendalwar, K Kielbasinski…

Index: Synthetic Communications, , vol. 20, # 12 p. 1877 - 1884

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Citation Number: 7

Abstract

SYNTHETIC COMMUNICATIONS, 20(12), 1877-1884 (1990 ... The enediol 7 l1 (230 mg) was treated with TMSI by the general procedure under nitrogen for 1 h. The crude product was purified by radial chromatography on silica gel, eluting with hexane-ethyl acetate (20:1), to ... Vol. ...