Tetrahedron letters

Resolution of 1, 3-alkanediols via chiral spiroketals derived from ℓ-menthone

T Harada, H Kurokawa, A Oku

Index: Harada, Toshiro; Kurokawa, Hideaki; Oku, Akira Tetrahedron Letters, 1987 ,  vol. 28,  # 41  p. 4843 - 4846

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Citation Number: 15

Abstract

Download full text in PDF Opens in a new window. Article suggestions will be shown in a dialog on return to ScienceDirect. ... Please enable JavaScript to use all the features on this page. ... Ketalization reaction of racemic 1,3-alkanediols with ℓ-menthone gave a mixture of diastereomeric spiroketals that was easily separated by silica gel column chromatography and converted into enantiomerically pure diols by acid-catalyzed hydrolysis. ... Reaction of racemic 1,3- ...