Inorganic chemistry

Reaction of m-terphenyldichlorophosphanes with sodium azide: Synthesis and characterization of stable azidocyclophosphazenes

RJ Wehmschulte, MA Khan, SI Hossain

Index: Al-Juaid, Salih S.; Dhaher, Saadi M.; Eaborn, Colin; Hitchcock, Peter B.; McGeary, Catherine A.; Smith J. David Journal of Organometallic Chemistry, 1989 , vol. 366, p. 39 - 52

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Citation Number: 36

Abstract

... m, broad), 6.76 (s, broad, 2H), 6.68 (td, 2H), J = 7.4, 2.4 Hz, 1.47 (s, broad, 18H), 1.33 (s, 36H), 1.23 ... 2127 (vs), 2142 (vs), 2151 (vs) cm - 1 . MS (FAB): m/z 1285.6 (M + H + , 19.2%), 1257.5 (M − N 2 ... Method B. Solid NaN 3 (1.30 g, 20 mmol) was added to a slurry of 2 (0.48 g, 1.1 ...