View all references we herein report the extension of this sulfone??based chemistry to a convenient, traceless, solid??phase synthesis of cycloalkylphosphonates and 1??cycloalkenylphosphonates using polystyrene??supported phenylsulfonylmethylphosphonate. The procedure for the synthesis of target compounds from polystyrene/1% divinylbenzene sodium phenylsulfinate (1) include (a) sulfinate S??alkylation, (b) the sulfonyl anion bis??alkylations with dihaloalkanes, and (c) ...
