New syntheses and molecular structures of the decamethylmetallocene dicarbonyls (. eta. 5-C5Me5) 2M (CO) 2 (M= titanium, zirconium, hafnium)

…, MD Rausch, RD Rogers, JL Atwood

Index: Sikora, David J.; Rausch, Marvin D.; Rogers, Robin D.; Atwood, Jerry L. Journal of the American Chemical Society, 1981 , vol. 103, p. 1265 - 1267

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Citation Number: 77

Abstract

Figure 1. ORTEP plot of the complex [(CH3)4N]+[(C7H,S2)2SnCI]- ... Figure 2. ORTEP plot of [(C2H5)4N]+[(C7H6S2)Ph2SnC1]- ... (6) The function minimized was Zw(lF.,l- lF,1)2. Mean atomic scattering factors were taken from ref 5, Vol. IV, 1974, pp 72-98. Real and imaginary dispersion corrections for Sn, C1, and S were taken from the same source, pp (7) Holmes, RR; Deiters, JA J. Am. Chem. SOC. 1977, 99, 3318. (8) Holmes, RR Acc. Chem. Res. 1979, 12, 257. 149- ...