Preparation of [carboxy??13C] 4??nitrophenylacetic acid

JET Corrie, VRN Munasinghe

Index: Corrie, John E. T.; Ranjit; Munasinghe Journal of Labelled Compounds and Radiopharmaceuticals, 2005 , vol. 48, # 3 p. 231 - 233

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Abstract

Abstract Reaction of sodium [13 C] cyanide with excess benzyl chloride gave∼ 75% utilization of the isotope. Subsequent nitration, isomer separation and hydrolysis of the nitrile gave the required carboxy-labelled 4-nitrophenylacetic acid. Copyright© 2005 John Wiley & Sons, Ltd.