The glyceryl unit is one of the simplest trifunctionalized molecules. The preparation of compounds bearing a single glyceryl unit at each dendrimeric terminus such as 1 has been reported 2 (Figure [1] ). In contrast, compounds such as 2, which bear repetitive branched glyceryl (BGL) units, have not been reported except in our previous papers dealing with BGL. [3] It is often difficult to create ether linkage in high yield (especially at sterically hindered positions) since the alkoxy ...