The Journal of Organic Chemistry

Notes. Synthesis of the Sulfur Analogs of Batyl and Chimyl Alcohols

D Lawson, H Getz, D Miller

Index: Lawson,D.D. et al. Journal of Organic Chemistry, 1961 , vol. 26, p. 615 - 616

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Citation Number: 10

Abstract

The following examples are given to illustrate the methods used to prepare the compounds listed in Tables I and TI. In general the experimental details varied very little from preparation to preparation. 4-Chloroisatoic anhydride. Phosgene was bubbled at mom temperature through a solution of 85.8 g.(0.500 mole) of 4chloroanthranilic acid'and 33.5 g.(0.316 mole) of sodium carbonate in 1750 ml. of water. The pH of the reaction mixture was maintained ...