Journal of the American Chemical Society

THE NITRATION OF 1, 1'-BINAPHTHYL

CS Schoepfle

Index: Schoepfle Journal of the American Chemical Society, 1923 , vol. 45, p. 1571

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Citation Number: 10

Abstract

The Acid from the Polymerized Ester.-The polymerized ester was hydrolyzed by dissolving it in 15 parts of acetone and adding to the boiling solution 5 equivalents, based on the monomolecular ester, of alcoholic potassium hydroxide. The latter was added, drop by drop, at such a rate that the material remained in solution continually during the hydrolysis. After the mixture had been heated for 6 hours about */a of the solvent was removed by distillation, the solution diluted ...