Method B.-A mixture consisting of 0.15 mole of the ethyl or methyl ether of 2-bromo-1- phenylethanol and 0.30 mole of the amine was heated under reflux in an oil-bath until an exothermic reaction occurred (Method B-1). When the reaction had abated somewhat, the mixture was then refluxed from one-half to 23 hours. The length of the heating period depended upon the amount of visible decomposition. In some cases the two reactants ...
