European Journal of Inorganic Chemistry

Two??and Three??Dimensional Hydrogen??Bonded Networks Built from 1, 3, 5??[(HO) 2 (O) P] 3C6H3 and 4??(Dimethylamino) pyridine

M Mehring

Index: Mehring, Michael European Journal of Inorganic Chemistry, 2004 , # 16 p. 3240 - 3246

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Citation Number: 20

Abstract

Abstract Crystallisation of 3, 5-bis (phosphonophenyl) phosphonic acid, 1, 3, 5-[(HO) 2 (O) P] 3 C 6 H 3, from MeOH/H 2 O in the presence of 4-(dimethylamino) pyridine, 4-(Me 2 N) C 5 H 4 N, gave [1-{(HO) 2 (O) P}-3, 5-{(HO)(O) 2 P} 2 C 6 H 3] 2−[{4-(Me 2 N) C 5 H 4 NH}+] 2 (2) and [1, 3-{(HO) 2 (O) P} 2-5-{(HO)(O) 2 P} C 6 H 3]−[4-(Me 2 N) C 5 H 4 NH]+(3). Single- crystal X-ray diffraction analyses revealed a two-and a three-dimensional hydrogen- ...