Aniline alkylation with di-and tribromopropane

VM Ismailov, IA Mamedov, NN Yusubov

Index: Ismailov; Mamedov; Yusubov Russian Journal of Organic Chemistry, 2009 , vol. 45, # 8 p. 1250 - 1251

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Abstract

At excess K2CO3 in DMSO environment the condensation of aniline (I) with 1, 3- dibromopropane (II) at heating (60–80 C) led to the formation of N-(3-bromopropyl)-aniline (III) and N-phenylazetidine (IV). At higher temperature the fraction of the cyclic product increased.