Synthesis and spectral study of a novel distamycin conjugate

MJ Pineda de las Infantas, J Campos…

Index: Pineda De Las Infantas; Campos; Baraldi; Romagnoli; Gallo; Espinosa Magnetic Resonance in Chemistry, 2003 , vol. 41, # 6 p. 478 - 480

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Abstract

Abstract The 1 H and 13 C NMR resonances for a novel distamycin conjugate, 3-[1-methyl-4- [1-methyl-4-[1-methyl-4-[N 1-[5-methyl-2, 4 (1H, 3H) pyrimidinedione] acetylamino] pyrrole-2- carboxamido] pyrrole-2-carboxamido] pyrrole-2-carboxamido] propionamidine hydrochloride (1), were assigned, using the concerted application of one-and two- dimensional NMR techniques including nuclear Overhauser effect difference, DEPT, ...