e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521
Reaction of 4-ethoxycarbonyl-2-phenyl-4, 5-dihydrooxazol-5-one with organolead (IV) triacetates. A route to some α-arylglycine and α-vinylglycine derivatives
MJ Koen, JT Pinhey, CJ Sherry
Index: Koen, Mark J.; Morgan, Jacqueline; Pinhey, John T.; Sherry, Christopher J. Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 4 p. 487 - 491
4-Ethoxycarbonyl-2-phenyl-4, 5-dihydrooxazol-5-one undergoes rapid arylation and vinylation with arylead triacetates and (E)-styryllead triacetates, respectively. The resulting moisture-sensitive 4-aryl-and 4-styryl-oxazolones undergo hydrolysis and decarboxylation under mild conditions to provide a short efficient route to derivatives of α-arylglycines and α- vinylglycines.