The Synthesis of Some Amino Alcohols

RE Holmen, DD Carroll

Index: Holmen; Carroll Journal of the American Chemical Society, 1951 , vol. 73, p. 1859

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Abstract

4-Anilino-1-butanol (a) From Tetramethylene Chlorohydrin.-Aniline (93 g., 1 mole), tetramethylene chlorohydrin (54.25 g., 0.5 mole) and benzene (100 ml.) were refluxed for 26 hours in a 500-d. round-bottom flask equipped with a suitable condenser. At the end of this time the supernatant liquid was decanted from the precipitate of aniline hydrochloride and combined with a little benzene used to rinse this precipitate. After distillation of the ...