Preparation and synthetic utility of phase-transfer catalysts anchored to polystyrene

MS Chiles, DD Jackson, PC Reeves

Index: Chiles, Margaret Shea; Jackson, Donald D.; Reeves, Perry C. Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2915 - 2918

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Citation Number: 53

Abstract

Org. Chem. 1978, 43, 4509. mL of 50% tert-butyl alcohol-doubly distilled water was added sodium hydroxide (1.517 g, 38 mmol), and the system was degassed and then constantly swept with nitrogen free of oxygen, under magnetic stirring. This was followed by the addition of bromobenzene (1 mL, 9.5 mmol) and toluene (0.5 mL) as internal standard. A 2- mL aliquot was removed at different reaction times to check the toluene/bromobenzene ...