Electroorganic chemistry. 59. Electroreductive synthesis of oximes from nitroolefins

…, H Hamaguchi, H Mikami, H Nogusa…

Index: Shono, Tatsuya; Hamaguchi, Hiroshi; Mikami, Hiroshi; Nogusa, Hideo; Kashimura, Shigenori Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2103 - 2105

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Citation Number: 14

Abstract

4 C, H,(CH,), CH= CHNO, C, H,(CH,), CH= NOH 17 C, H,(CH,), CH (OCH,), 23 40 a See ref 8 and 9. Isolated yield. some operation.'Preparation of nitro olefins from al- Scheme I dehydes and nitroalkanes and subsequent reduction with reducing agents such as titanium trichloride seem to be a reliable method for synthesis of oximes (Scheme 1): while the use of titanium trichloride as the reducing agent often technique. On the other hand, a variety of ...