e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521
ω-Hydroxy-1-alkanesulfonyl chlorides
JF King, MR Webster, N Chiba, JK Allen…
Index: King, J. F.; Webster, Michael R.; Chiba, Naoki; Allen, Julie K.; Parker, Kenneth J. M.; et al. Phosphorus and Sulfur and the Related Elements, 1987 , vol. 31, p. 161 - 176
Abstract The general synthesis of hydroxyalkanesulfonyl chlorides is illustrated by the preparation of 6-hydroxy-1-butanesulfonyl chloride (2e) and 5-hydroxy-1-pentanesulfonyl chloride (2d) as fairly stable, oily liquids (of∼ 95% purity) characterized by 1Hmr, 13Cmr and infrared spectra, and by conversion both to the corresponding sultones (3) and to crystalline acetoxy-piperidides (6); 2d and 2e form apparent polymers, very slowly on ...
