The reaction of organic halides with piperidine. IV. Bromo esters

WV Drake, SM McElvain

Index: Drake; McElvain Journal of the American Chemical Society, 1934 , vol. 56, p. 698

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Citation Number: 12

Abstract

20 g. of 2, 4, 6-tribromobenzene, 30 cc. of chlorosulfonic acid and 30 CC. of sulfuryl chloride was heated at 100'for four hours. The reaction mixture was worked up by the iame procedure as above. The yield was 15-19 g.(57-ETo) of a buff colored product which melted at 63.5-64".