(q), 26.8 (q), 17.9 (q), 17.6 (t), 17.6 (q); HRMS obsd m/z 263.1703, C16H25NS requires 263.1709. Single-Crystal X-ray Diffraction Analysis of 5. A suitable single crystal was glued to a glass fiber, and preliminary X-ray photographs were taken. Compound 5 had orthorhombic sym- metry with a = 9.543 (2), b = 10.371 (2), and c = 15.373 (3) A. Systematic absences, a calculated density, and the compound's optical activity were uniquely accommodated by space ...
[Sander, Wolfram; Strehl, Anja; Maguire, Anita R.; Collins, Stuart; Kelleher, Patrick G. European Journal of Organic Chemistry, 2000 , # 19 p. 3329 - 3335]