Tetrahedron letters

Diastereoselective radical alkylations of alkyl aryl sulfoxides

…, G Caron, PA Carrupt, N Knouzi, P Renaud

Index: Zahouily, Mohamed; Caron, Giulia; Carrupt, Pierre-Alain; Knouzi, Nourdine; Renaud, Philippe Tetrahedron Letters, 1996 , vol. 37, # 46 p. 8387 - 8390

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Citation Number: 16

Abstract

) and were further purified by flash chromatography. All new compounds have been characterized by 1 H-NMR, 13 C-NMR. MS, IR and elemental analysis. : 1 H-NMR (250 MHz, CDCl 3 ): 7.44–7.55 (m, 5H); 6.03 (d, J = 0.5, 1H); 5.50 (qdm, J = 6.7, 2.8, 1H); 3.50 (s, 3H); 2.75 (ddd, J = 10.3, 5.1, 3.5, 1H); 2.50–2.65 (m, 1H); 2.06–2.25 (qdm, J = 6.7, 2.8, 1H); 1.23 (d, J = 6.8, 3H); 1.18 (d, J = 6.9, 3H). : 7.45–7.60 (m, 5H); 6.18 (d, J = 0.5, 1H); 5.62 (d, J = 0.5, 1H); ...