GaCl3-Assisted cyclization reactions in hypersilyl (trimethylsilyl) aminodichlorophosphine

A Villinger, A Westenkirchner, R Wustrack…

Index: Neemann, Jutta; Klingebiel, Uwe Chemische Berichte, 1981 , vol. 114, # 2 p. 527 - 535

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Citation Number: 16

Abstract

... amide is formed in situ by the addition of n-BuLi in n-hexane at 0 °C. (ii) The reaction ... The solvent volume was then reduced to incipient crystallization in vacuo, and the solution was stored at −20 °C for ... of a cyclo-2-phospha-4-sila-1,3-diazenium salt [Me 2 Si(N-t-Bu) 2 P + AlC1 4 ...