Fully enzymatic resolution of chiral amines: acylation and deacylation in the presence of Candida antarctica lipase B

H Ismail, RM Lau, F van Rantwijk…

Index: Advanced Synthesis and Catalysis, , vol. 350, # 10 p. 1511 - 1516

Full Text: HTML

Citation Number: 40

Abstract

... Keywords: amines; Candida antarctica lipase B; enantioselective acylation; enzymatic deacylation; enzyme catalysis Introduction ... All other compounds were purchased from ACROS and Sigma or synthesized as described below. Enzyme Assays ... Synthesis of Acyl Donors ...

 Related Synthetic Route
(R)-N-(heptan-2-yl)-2-(methylthio)acetamide Structure

1056469-62-5

(R)-N-(heptan-2...

~%

(METHYLTHIO)ACETICACID Structure

2444-37-3

(METHYLTHIO)ACE...

2-Aminoheptane Structure

123-82-0

2-Aminoheptane

(R)-N-(2-heptyl)-2-methoxyacetamide Structure

1056469-59-0

(R)-N-(2-heptyl...

~%

2-Aminoheptane Structure

123-82-0

2-Aminoheptane

2-Methoxyacetic acid Structure

625-45-6

2-Methoxyacetic acid

2-methoxy-N-[(1R)-1-phenylethyl]acetamide Structure

162929-44-4

2-methoxy-N-[(1...

~%

(R)-(+)-1-Phenylethylamine Structure

3886-69-9

(R)-(+)-1-Pheny...

2-Methoxyacetic acid Structure

625-45-6

2-Methoxyacetic acid

(R)-N-(heptan-2-yl)-2-(methylamino)acetamide Structure

1056469-56-7

(R)-N-(heptan-2...

~%

Sarcosine Structure

107-97-1

Sarcosine

2-Aminoheptane Structure

123-82-0

2-Aminoheptane

(R)-2-(methylamino)-N-(1-phenylethyl)acetamide Structure

1056469-66-9

(R)-2-(methylam...

~%

Sarcosine Structure

107-97-1

Sarcosine

(R)-(+)-1-Phenylethylamine Structure

3886-69-9

(R)-(+)-1-Pheny...

2-phenoxy-N-[(R)-1-phenylethyl]acetamide Structure

1056469-95-4

2-phenoxy-N-[(R...

~%

(R)-(+)-1-Phenylethylamine Structure

3886-69-9

(R)-(+)-1-Pheny...

Phenoxyacetic acid Structure

122-59-8

Phenoxyacetic acid

(R)-N-(heptan-2-yl)-2-phenoxyacetamide Structure

1056469-88-5

(R)-N-(heptan-2...

~%

2-Aminoheptane Structure

123-82-0

2-Aminoheptane

Phenoxyacetic acid Structure

122-59-8

Phenoxyacetic acid

N/A Structure

1056469-90-9

N/A

~%

Phenyl thioacetic acid Structure

103-04-8

Phenyl thioacet...

2-Aminoheptane Structure

123-82-0

2-Aminoheptane

(R)-N-(1-phenylethyl)-2-(phenylthio)acetamide Structure

1056469-97-6

(R)-N-(1-phenyl...

~%

Phenyl thioacetic acid Structure

103-04-8

Phenyl thioacet...

(R)-(+)-1-Phenylethylamine Structure

3886-69-9

(R)-(+)-1-Pheny...

N/A Structure

1056469-86-3

N/A

~%

2-Aminoheptane Structure

123-82-0

2-Aminoheptane

N-Phenylglycine Structure

103-01-5

N-Phenylglycine

N/A Structure

1056469-93-2

N/A

~%

(R)-(+)-1-Phenylethylamine Structure

3886-69-9

(R)-(+)-1-Pheny...

N-Phenylglycine Structure

103-01-5

N-Phenylglycine


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