Tetrahedron letters

Microwave-assisted clean synthesis of 6-aryl-2, 4-diamino-1, 3, 5-triazines in [bmim][PF 6]

Y Peng, G Song

Index: Peng, Yanqing; Song, Gonghua Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5313 - 5316

Full Text: HTML

Citation Number: 36

Abstract

An efficient and green approach was developed to prepare 6-aryl-2, 4-diamino-1, 3, 5- triazines from corresponding arylnitriles and dicyanodiamide in ionic liquid [bmim][PF6] under computer-controlled microwave irradiation. Particularly valuable features of this method included the short reaction time, good yield, convenient operation and eco-friendly solvent.