REACTIONS OF AMINES. IX. THE REARRANGEMENT OF Nt-BUTYL-N-CHLOROAMIDES1-2

HE Baumgarten, RL Zey, U Krolls

Index: Baumgarten,H.E. et al. Journal of the American Chemical Society, 1961 , vol. 83, p. 4469 - 4470

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Citation Number: 20

Abstract

Fig. 1.-Infrared spectra:, 4, saturated solution of Ia in benzene (benzene peaks at 5.09 p and 5.51 p); B, after addition of 1 equiv. of t-butyl hypochlorite and 0.5 equiv. of potassium t- butoxide; C, after addition of l equiv. of potassium t-butoxide; D, after addition of slightly more than 1 equiv. of potassium t-butoxide; E, after evaporation of solution of curve C to dryness and extraction of solids with pentane; F, mixture of curve E after two weeks in freezer. ...