Synthetic communications

A rapid and efficient synthesis of symmetrical disulfides under microwave irradiation conditions

JX Wang, L Gao, D Huang

Index: Wang, Jin-Xian; Gao, Lijuan; Huang, Danfeng Synthetic Communications, 2002 , vol. 32, # 7 p. 963 - 969

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Citation Number: 28

Abstract

ABSTRACT A rapid and general method for the synthesis of symmetrical disulfides involves reaction of sulfur with sodium hydroxide under PTC-microwave irradiation condition to give sodium disulfide, which reacts with alkyl halides to afford the disulfides in good to excellent isolated yields.

~92%

~85%

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