The Journal of Organic Chemistry

2, 3-Bis (trimethylsilyloxy)-1, 3-butadiene as a useful reactive diene in the Diels-Alder reaction

DR Anderson, TH Koch

Index: Anderson,D.R.; Koch,T.H. Journal of Organic Chemistry, 1978 , vol. 43, p. 2726 - 2728

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Citation Number: 28

Abstract

GC analyses were performed on a Perkin-Elmer F 11 gas chromatograph equipped with a column of 2% OV 17 (2 m X 2 mm). Absolute yields have been evaluated by comparison of the peaks of the reaction mixture with those of standard solutions. Infrared spectra (in CC14) were obtained on a Perkin-Elmer 257 Infracord instrument. Nuclear magnetic resonance spixtra were recorded on a Perkin-Elmer R32 90 MHz spectrometer, using Me4Si as an ...