Pheromone, XXVIII. Stereoselektive Synthese (E)??olefinischer Schmetterlingspheromone

…, T Röder, O Vostrowsky, HJ Bestmann

Index: Canevet; Roeder; Vostrowsky; Bestmann Chemische Berichte, 1980 , vol. 113, # 3 p. 1115 - 1120

Full Text: HTML

Citation Number: 19

Abstract

Abstract Es wird eine allgemeine stereoselektive Synthese (E)-konfigurierter mono- olefinischer Pheromone und deren Strukturabwandlungsprodukte durch Alkylierung von Allyldiethylphosphonaten und nachfolgende Reduktion mit Lithiumaluminiumhydrid beschrieben.

 Related Synthetic Route
2-[(10-bromodecyl)oxy]tetrahydro-2H-pyran Structure

51795-88-1

2-[(10-bromodec...

~%

trans-11-tetradecenyl acetate Structure

33189-72-9

trans-11-tetrad...

diethyl (14-((tetrahydro-2H-pyran-2-yl)oxy)tetradec-2-en-4-yl)phosphonate Structure

57586-82-0

diethyl (14-((t...

~%

trans-11-tetradecenyl acetate Structure

33189-72-9

trans-11-tetrad...

(E)-1-(2-tetrahydropyranyloxy)-7-decene Structure

73881-17-1

(E)-1-(2-tetrah...

~%

acetic acid,dec-7-en-1-ol Structure

13857-04-0

acetic acid,dec...

2-(6-Bromohexyloxy)tetrahydropyran Structure

53963-10-3

2-(6-Bromohexyl...

~%

acetic acid,dec-7-en-1-ol Structure

13857-04-0

acetic acid,dec...

diethyl (10-((tetrahydro-2H-pyran-2-yl)oxy)dec-2-en-4-yl)phosphonate Structure

73881-12-6

diethyl (10-((t...

~%

acetic acid,dec-7-en-1-ol Structure

13857-04-0

acetic acid,dec...

(2E)-1-Bromo-2-octene Structure

56318-83-3

(2E)-1-Bromo-2-...

~%

(E)-7-Tetradecen-1-ol Structure

37011-95-3

(E)-7-Tetradece...

Trans-2-Octen-1-ol Structure

18409-17-1

Trans-2-Octen-1-ol

~%

(E)-7-Tetradecen-1-ol Structure

37011-95-3

(E)-7-Tetradece...

METHYL TRANS-2-OCTENOATE Structure

7367-81-9

METHYL TRANS-2-...

~%

(E)-7-Tetradecen-1-ol Structure

37011-95-3

(E)-7-Tetradece...

Hexanal Structure

66-25-1

Hexanal

~%

(E)-7-Tetradecen-1-ol Structure

37011-95-3

(E)-7-Tetradece...

(E)-2-octenylphosphonic acid diethyl ester Structure

73881-09-1

(E)-2-octenylph...

~%

(E)-7-Tetradecen-1-ol Structure

37011-95-3

(E)-7-Tetradece...

diethyl (1-((tetrahydro-2H-pyran-2-yl)oxy)tetradec-8-en-7-yl)phosphonate Structure

73881-15-9

diethyl (1-((te...

~%

(E)-7-Tetradecen-1-ol Structure

37011-95-3

(E)-7-Tetradece...

Hexanal Structure

66-25-1

Hexanal

Methyl triphenylphosphoranylideneacetate Structure

21204-67-1

Methyl tripheny...

~82%

METHYL TRANS-2-OCTENOATE Structure

7367-81-9

METHYL TRANS-2-...

2-(6-Bromohexyloxy)tetrahydropyran Structure

53963-10-3

2-(6-Bromohexyl...

~%

dec-7-en-1-ol Structure

52957-12-7

dec-7-en-1-ol

diethyl (10-((tetrahydro-2H-pyran-2-yl)oxy)dec-2-en-4-yl)phosphonate Structure

73881-12-6

diethyl (10-((t...

~%

dec-7-en-1-ol Structure

52957-12-7

dec-7-en-1-ol

diethyl (12-((tetrahydro-2H-pyran-2-yl)oxy)dodec-4-en-6-yl)phosphonate Structure

73881-13-7

diethyl (12-((t...

~%

2-[(E)-7-Dodecenyloxy]tetrahydro-2H-pyran Structure

55305-37-8

2-[(E)-7-Dodece...

1-bromohex-2-ene Structure

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1-bromohex-2-ene

~%

2-[(E)-7-Dodecenyloxy]tetrahydro-2H-pyran Structure

55305-37-8

2-[(E)-7-Dodece...

Diethyl-(E)-2-hexenylphosphonat Structure

73881-08-0

Diethyl-(E)-2-h...

~%

2-[(E)-7-Dodecenyloxy]tetrahydro-2H-pyran Structure

55305-37-8

2-[(E)-7-Dodece...

2-(8-bromooctoxy)oxane Structure

50816-20-1

2-(8-bromooctox...

~%

trans-9-dodecen-1-ol Structure

35237-62-8

trans-9-dodecen-1-ol

diethyl (12-((tetrahydro-2H-pyran-2-yl)oxy)dodec-2-en-4-yl)phosphonate Structure

73881-14-8

diethyl (12-((t...

~%

trans-9-dodecen-1-ol Structure

35237-62-8

trans-9-dodecen-1-ol

2-(5-bromopentoxy)oxane Structure

37935-47-0

2-(5-bromopento...

~%

(Z)-6-nonen-1-ol Structure

31502-19-9

(Z)-6-nonen-1-ol

diethyl (9-((tetrahydro-2H-pyran-2-yl)oxy)non-2-en-4-yl)phosphonate Structure

73881-11-5

diethyl (9-((te...

~%

(Z)-6-nonen-1-ol Structure

31502-19-9

(Z)-6-nonen-1-ol

2-(5-bromopentoxy)oxane Structure

37935-47-0

2-(5-bromopento...

(E)-diethyl but-2-en-1-ylphosphonate Structure

26327-86-6

(E)-diethyl but...

Ethanoic anhydride Structure

108-24-7

Ethanoic anhydride

~%

2-fluoro-3-phenylbut-2-enoyl fluoride Structure

55305-36-7

2-fluoro-3-phen...

Detail
2-[(E)-9-Dodecenyloxy]tetrahydro-2H-pyran Structure

71566-57-9

2-[(E)-9-Dodece...

~%

TRANS-9-DODECEN-1-YL ACETATE Structure

35148-19-7

TRANS-9-DODECEN...

2-(8-bromooctoxy)oxane Structure

50816-20-1

2-(8-bromooctox...

~%

TRANS-9-DODECEN-1-YL ACETATE Structure

35148-19-7

TRANS-9-DODECEN...

diethyl (12-((tetrahydro-2H-pyran-2-yl)oxy)dodec-2-en-4-yl)phosphonate Structure

73881-14-8

diethyl (12-((t...

~%

TRANS-9-DODECEN-1-YL ACETATE Structure

35148-19-7

TRANS-9-DODECEN...

2-[(10-bromodecyl)oxy]tetrahydro-2H-pyran Structure

51795-88-1

2-[(10-bromodec...

~%

e-11-tetradecen-1-ol Structure

35153-18-5

e-11-tetradecen-1-ol

diethyl (14-((tetrahydro-2H-pyran-2-yl)oxy)tetradec-2-en-4-yl)phosphonate Structure

57586-82-0

diethyl (14-((t...

~%

e-11-tetradecen-1-ol Structure

35153-18-5

e-11-tetradecen-1-ol

9E-Hexadecen-1-ol Structure

64437-47-4

9E-Hexadecen-1-ol

Ethanoic anhydride Structure

108-24-7

Ethanoic anhydride

~85%

9E-Hexadecenyl Acetate Structure

56218-69-0

9E-Hexadecenyl ...

(2E)-1-Bromo-2-octene Structure

56318-83-3

(2E)-1-Bromo-2-...

~%

9E-Hexadecenyl Acetate Structure

56218-69-0

9E-Hexadecenyl ...

Trans-2-Octen-1-ol Structure

18409-17-1

Trans-2-Octen-1-ol

~%

9E-Hexadecenyl Acetate Structure

56218-69-0

9E-Hexadecenyl ...

METHYL TRANS-2-OCTENOATE Structure

7367-81-9

METHYL TRANS-2-...

~%

9E-Hexadecenyl Acetate Structure

56218-69-0

9E-Hexadecenyl ...

Hexanal Structure

66-25-1

Hexanal

~%

9E-Hexadecenyl Acetate Structure

56218-69-0

9E-Hexadecenyl ...

(E)-2-octenylphosphonic acid diethyl ester Structure

73881-09-1

(E)-2-octenylph...

~%

9E-Hexadecenyl Acetate Structure

56218-69-0

9E-Hexadecenyl ...

diethyl (16-((tetrahydro-2H-pyran-2-yl)oxy)hexadec-6-en-8-yl)phosphonate Structure

73881-16-0

diethyl (16-((t...

~%

9E-Hexadecenyl Acetate Structure

56218-69-0

9E-Hexadecenyl ...

(E)-2-(hexadec-9-en-1-yloxy)tetrahydro-2H-pyran Structure

73881-18-2

(E)-2-(hexadec-...

~%

9E-Hexadecenyl Acetate Structure

56218-69-0

9E-Hexadecenyl ...

1-bromohex-2-ene Structure

73881-10-4

1-bromohex-2-ene

~%

(E)-Dodec-7-en-1-ol Structure

16695-40-2

(E)-Dodec-7-en-1-ol

Diethyl-(E)-2-hexenylphosphonat Structure

73881-08-0

Diethyl-(E)-2-h...

~%

(E)-Dodec-7-en-1-ol Structure

16695-40-2

(E)-Dodec-7-en-1-ol

diethyl (12-((tetrahydro-2H-pyran-2-yl)oxy)dodec-4-en-6-yl)phosphonate Structure

73881-13-7

diethyl (12-((t...

~%

(E)-Dodec-7-en-1-ol Structure

16695-40-2

(E)-Dodec-7-en-1-ol

METHYL TRANS-2-OCTENOATE Structure

7367-81-9

METHYL TRANS-2-...

~41%

Trans-2-Octen-1-ol Structure

18409-17-1

Trans-2-Octen-1-ol


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