Synlett

Copper-Catalyzed Aromatic CH Bond Halogenation Using Lithium Halides as Halogenating Reagents

Y Lu, R Wang, X Qiao, Z Shen

Index: Synlett, , # 7 p. 1038 - 1042

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Citation Number: 13

Abstract

... Synlett 2011(7): 1038 ... 8, K 2 S 2 O 8, 48, nr, nr. 9, Oxone, 48, 7, -. ... 11 e, CrO 3, 48, -, 71 f. a Reaction conditions: 1 (30 mg, 0.19 mmol), LiCl (33 mg, 0.77 mmol), Cu(NO 3 ) 2 ˙3H 2 O (9.4 mg, 20 mol%), Ph 3 P (20.3 mg, 40 mol%), AcOH (1.5 mL), 150 ˚C, oxidant (4 equiv), in a sealed ...