Journal of organometallic chemistry

Procedures for the preparation of silanols

JA Cella, JC Carpenter

Index: Cella, James A.; Carpenter, John C. Journal of Organometallic Chemistry, 1994 , vol. 480, # 1-2 p. 23 - 26

Full Text: HTML

Citation Number: 50

Abstract

Abstract Two procedures are described for the preparation of silanols and silanediols from the corresponding chlorosilanes. The first procedure, a two-phase hydrolysis-extraction process, is particularly convenient and suited to the preparation of a wide range of mono- silanols. Hydrolysis of dichlorosilanes by this procedure gives varied results depending on the structure of the dichlorosilane and specific reaction conditions. The second procedure, ...