Preparation and nmr-spectral characteristics of benzyl-α, α-d2 ethers of monosaccharides

A Zamojski, B Grzeszczyk, A Banaszek, J Babiński…

Index: Zamojski, Aleksander; Grzeszczyk, Barbara; Banaszek, Anna; Babinski, Jakub; Bordas, Xavier; et. al. Carbohydrate Research, 1985 , vol. 142, p. 165 - 171

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Citation Number: 4

Abstract

R= PhCD,'or 3D-10D 1 consisting in reduction of qa, a-trichlorotoluene with zinc-acetic acid- d,(AcOD) to toluene-a, cY, cY-d3, and bromination of the latter. In our method6, sodium phenylacetate is refluxed with 1520% sodium deuteroxide in deuterium oxide until the desired degree of H+= D exchange has