Alkylation of allylic derivatives. 11. Copper (I)-catalyzed cross coupling of allylic carboxylates with Grignard reagents

CC Tseng, SD Paisley, HL Goering

Index: Tseng, Chung Chyi; Paisley, Steven D.; Goering, Harlan L. Journal of Organic Chemistry, 1986 , vol. 51, # 15 p. 2884 - 2891

Full Text: HTML

Citation Number: 112

Abstract

3-OTMB 4 these experiments and reaction mixtures were prepared and stirred for 5 h at 0 OC. 12 Yields of isolated products (4) are shown in Table I. Ranges are given for cases with two or more independent experiments. Except as noted, isolated products were shown to be homogeneous by capillary GC and were identified by IR and NMR spectra and GC retention times.