The Journal of Organic Chemistry

Poly (ethylene glycols) are extraordinary catalysts in liquid-liquid two-phase dehydrohalogenation

Y Kimura, SL Regen

Index: Kimura, Yoshikazu; Regen, Steven L. Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2493 - 2494

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Citation Number: 69

Abstract

Communtcattons with a No-Air stopper. Then the mixture was heated with stirring for 8 h at 100 OC. The reaction mixture was filtered to remove Pd metal and K2S208, was neutralized with saturated aqueous sodium bicarbonate, and was extracted with ether. After evaporation of the ether, the products were analyzed by GLC and, in some cases, separated by column chromatography (silica gel). Yields were determined by GLC directly with the use of an ...