Synthetic communications

Improved procedures for the preparation of 2-nitro-5-methoxyphenol and 6-methoxy-2 (3H)-benzoxazolone from 3-methoxyphenol

RJ Maleski

Index: Synthetic Communications, , vol. 23, # 3 p. 343 - 348

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Citation Number: 13

Abstract

SYNTHETIC COMMUNICATIONS, 23(3), 343-348 (1993 ... 2-Nitroso-5-Methoxv~henol (2) A solution of 12.4 g ( 0.1 mole) of 3- rnethoxyphenol (Aldrich) in 100 mL of ... product was filtered and washed with 60 mL of 50% aqueous propionic acid, and then with a lar e volume of water ...