ELEMENTORGANISCHE VERBINDUNGEN MIT O-PHENYLENSUBSTITUENTEN, XX, 1 2, 3, 7, 8-TETRA (METHYLTHIO) THIANTHREN

M Dötze, G Klar

Index: Doetze, Marc; Klar, Guenter Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 63, # 1/2 p. 217 - 222

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Abstract

Abstract Starting from thiophenol (3) the sequence 1, 2-di (methylthio) benzene (4)→ 1- bromo-3, 4-di (methylthio) benzene (5)→ bis [3, 4-di (methylthio) phenyl] sulfide (6)→ bis [2- bromo-4, 5-di (methylthio) phenyl]-sulfide (7) finally leads to the title compound 2). The 1H and 13C-NMR, and the MS data of 2 are reported. The 1H-NMR data of compounds 5–7 are also given. Ausgehend von Thiophenol (3) kommt man über die Zwischenstufen 1, 2-Di ( ...

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