Chemische Berichte

LiClO4??Promoted Addition of Alkyl Grignard and Alkynyllithium Reagents to Ketones. Comparison of a 5 M LiClO4/Diethyl Ether Solution with CeCl3

J Ipaktschi, T Eckert

Index: Chemische Berichte, , vol. 128, # 12 p. 1171 - 1174

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Citation Number: 16

Abstract

... (C), 122.70 (C), 126.94 (2 X CH), 128.03 (4 X CH), 128. ... 7 H20 (Fluka) was dried at 140°C and 0.5 Torr for 4 h, then cooled to 0°C and stirred with 4 ml of THF for 12 h. After addition of 1 mmol of the respective ketone in 2 ml of THF and stirring ofthe mixture for 2 h, 2 ... 1991, vol. ...