Synthesis and characterization of spiro [3.4] octa-5, 7-diene

RD Miller, M Schneider, DL Dolce

Index: Miller,R.D. et al. Journal of the American Chemical Society, 1973 ,  vol. 95, p. 8468 - 8469            

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Citation Number: 15

Abstract

The recent confirmation by photoelectron spectroscopy of direct interaction between the cyclopropane ring and the n-orbitals in spiro [2.4] hepta-4, 6-diene (1)'has rekindled interest in the properties of spirocyclopentadiene derivatives. Within the homologous series of spirodienes 1-3, spiro [3.4] octa-5, 7-diene (2) has until now escaped synthesis and characterization despite a number of reported attempts. 2, 3 This material by virtue of its ...