Chemical Communications

Nitration of cyclic vinylsilanes with acetyl nitrate: effect of silyl moiety and ring size

GS Patil, G Nagendrappa

Index: Patil, Govindagouda S.; Nagendrappa, Gopalpur Chemical Communications, 1999 , # 12 p. 1079 - 1080

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Citation Number: 7

Abstract

... Govindagouda S. Patil and Gopalpur ... 9 Selected data for 9: mp 56–58°C; nmax/cm21 1652, 1595, 1564; dH(CDCl3) 6.19 (dd, J 7.6 and 1.4, 1H), 2.94–2.63 (m, 2H), 2.45–2.30 (m, 1H), 2.12–1.99 (m, 1H), 1.89–1.77 (m, 4H), 1.59–1.44 (m, 4H); dC(CDCl3) 121.5 (s), 78.7 (d), 32.3 (t), 30.6 (t), 25.9 (t), 25.8 (t), 24.8 (t), 21.8 (t); dO(CDCl3) 596.3, 445.2, 352.9; m/z 264 (1%, M+ + 1), 171 (3), 95 (37), 81 (34), 67 (37), 55 (72), 46 (100, NO2 +), 41 (67) (Found: C ...