Self-assembling polycondensation was examined to prepare the whisker of poly (p- oxybenzoyl-alt-p-mercaptobenzoyl). Polymerizations were carried out in liquid paraffin (LPF) and aromatic solvents such as Therm S 800 and 1000 at 300° C for 6 h. Polymerization concentration was 1.0 wt/vol%. The whisker was not obtained by the random copolymerization of p-acetoxybenzoic acid and S-acetyl-4-mercaptobenzoic acid at the ...