Improved alkylation of ethyl acetoacetate and diethyl malonate

D Barbry, C Faven, A Ajana

Index: Organic Preparations and Procedures International, , vol. 26, # 4 p. 469 - 471

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Citation Number: 3

Abstract

... Thus, we investigated more convenient preparation techniques. ... General Procedure.- A mixture of 11.09 g of potassium carbonate (0.08 mol), 50 mL of water, 4.29 g of ethyl acetoacetate (0.033 mol), 4.00 g of ... The organic layers were dried over magnesium sulfate and distilled. ...