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e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521

Synlett

Oxidative deprotection of 1, 3-dithiane group using NaClO2 and NaH2PO4 in aqueous methanol

T Ichige, A Miyake, N Kanoh, M Nakata

Index: Synlett, , # 10 p. 1686 - 1690

Full Text: HTML

Citation Number: 16

Abstract

... p.2983-2989; 2e Yus M. Nájera C. Foubelo F. Tetrahedron 2003, 59: 6147; Our recent examples, see: 3a Ide M. Yasuda M. Nakata M. Synlett ... 2004, 126: 5192; 6s Ammonium persulfate on Montmorillonite K-10, microwave: Ganguly NC. Datta M. Synlett 2004, 659; 8a Lindgren BO ...

 Related Synthetic Route
Methanol Structure

67-56-1

Methanol

2-(3,4-DIMETHOXY-PHENYL)-[1,3]DITHIANE Structure

50766-67-1

2-(3,4-DIMETHOX...

~26%

Methyl 3,4-dimethoxybenzoate Structure

2150-38-1

Methyl 3,4-dime...

Veratric acid Structure

93-07-2

Veratric acid

veratraldehyde Structure

120-14-9

veratraldehyde

~%

Methyl 3,4-dimethoxybenzoate Structure

2150-38-1

Methyl 3,4-dime...

Methanol Structure

67-56-1

Methanol

4-Methoxybenzaldehyde trimethylenedithioacetal Structure

24588-72-5

4-Methoxybenzal...

~14%

Methyl anisate Structure

121-98-2

Methyl anisate

p-Anisic acid Structure

100-09-4

p-Anisic acid

S-(3-mercaptopropyl) 4-methoxybenzothioate Structure

769936-27-8

S-(3-mercaptopr...

~%

Methyl anisate Structure

121-98-2

Methyl anisate

Methanol Structure

67-56-1

Methanol

N/A Structure

156387-49-4

N/A

~%

Methyl anisate Structure

121-98-2

Methyl anisate

p-Anisic acid Structure

100-09-4

p-Anisic acid

Methanol Structure

67-56-1

Methanol

2-(3,4-DIMETHOXY-PHENYL)-[1,3]DITHIANE Structure

50766-67-1

2-(3,4-DIMETHOX...

~66%

Methyl 3,4-dimethoxybenzoate Structure

2150-38-1

Methyl 3,4-dime...

Veratric acid Structure

93-07-2

Veratric acid

Methanol Structure

67-56-1

Methanol

4-Methoxybenzaldehyde trimethylenedithioacetal Structure

24588-72-5

4-Methoxybenzal...

~70%

Methyl anisate Structure

121-98-2

Methyl anisate

p-Anisic acid Structure

100-09-4

p-Anisic acid

4-Methoxybenzaldehyde trimethylenedithioacetal Structure

24588-72-5

4-Methoxybenzal...

~%

4-Methoxybenzaldehyde Structure

123-11-5

4-Methoxybenzal...

p-Anisic acid Structure

100-09-4

p-Anisic acid

N/A Structure

156387-49-4

N/A

S-(3-mercaptopropyl) 4-methoxybenzothioate Structure

769936-27-8

S-(3-mercaptopr...

~%

p-Anisic acid Structure

100-09-4

p-Anisic acid

Methanol Structure

67-56-1

Methanol

N/A Structure

156387-49-4

N/A

~%

Methyl anisate Structure

121-98-2

Methyl anisate

p-Anisic acid Structure

100-09-4

p-Anisic acid

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Detail Synthetic Route


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