Reactions of 2-furyl, 2-thienyl, and N-methyl-2-pyrrolyl mercurials with [Et3NH][(. mu.-CO)(. mu.-RS) Fe2 (CO) 6] complexes. Synthesis of Fe2 (CO) 6 complexes with …

D Seyferth, LL Anderson, F Villafane, M Cowie…

Index: Seyferth, Dietmar; Anderson, Lea L.; Villafane, Fernando; Cowie, Martin; Hilts, Robert W. Organometallics, 1992 , vol. 11, p. 3262 - 3271

Full Text: HTML

Citation Number: 26

Abstract

Materials. Dichloromethaue (Fisher) was washed with fuming sulful.ic acid, water, and aqueous NaHC03 and then distilled twice from CaHz under nitrogen. Benzene (Fisher) was refluxed over and distilled from CaHz under nitrogen and stored over sodi- um/potaseium alloy. W ic acid (3M, Chemistry Division) was distilled under vacuum. Methylmagnesium bromide, 3.0 M in EhO (Aldrich) was used as received. Octaphenylcyclotetrasilane was prepared according to a ...