Russian journal of organic chemistry

Synthesis of 5 (6)-(4-aminophenythio)-2-aminobenzimidazole derivatives: III. Preparation procedure for 3, 4, 4'-triaminodiphenyl sulfide

VS Pilyugin, LV Yakovleva

Index: Pilyugin; Yakovleva Russian Journal of Organic Chemistry, 2002 , vol. 38, # 8 p. 1137 - 1141

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Citation Number: 1

Abstract

Abstract A procedure for preparation of 3, 4, 4'-triaminodiphenyl sulfide by reduction of 4- amino-3, 4'-dinitrodiphenyl sulfide with hydrazine hydrate in butanol catalyzed by a mixture of iron (III) chloride and activated carbon was developed providing the product in no less than 80% yield with the main compound content no less than 93%.