The Journal of Organic Chemistry

Synthesis and Properties of 5-(Substituted) Mercaptotetrazoles1

E Lieber, T Enkoji

Index: Lieber,E.; Enkoji,T. Journal of Organic Chemistry, 1961 , vol. 26, p. 4472 - 4479

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Citation Number: 50

Abstract

Improved procedure for the synthd of aryl thiocyanatm have been developed. A ceria of alkyl and aryl thiocyanakn has been converted to 5-(auhstituted) mercaptotetmwla by reaction with txside ion in dimethylfo" nide in the p-ce of ammonium chloride. The 5-(mbetituted) memaptotetramlea undergo decompoeition, at or near their melting pohb, to hydraGoic acid and the corresponding thiocyanate. The ultraviolet spectra indica-that the tetrrrsolyl sulfide ...

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