The Journal of Organic Chemistry

Ozonolysis of tetraphenylcyclopentadienone

PS Bailey, TM Ferrell

Index: Bailey, Philip S.; Ferrell, Thomas M. Journal of Organic Chemistry, 1981 , vol. 46, # 24 p. 5028 - 5030

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Citation Number: 4

Abstract

Experimental Section Ozonation of Tetraphenylcyclopentadienone (1). Ten millimoles of ozone was passed into a solution of 10 mmol of 1 (Aldrich, mp 217-220" C) in 100 mL of dichloromethane at-78" C by the usual procedure (earlier papers of senior author). The ozone absorption was generally quantitative and the reaction mixture changes from deep purple to light gold. The solvent wm removed via a rotary evaporator and the red-gold ...