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Phosphorus, Sulfur, and Silicon
Synthesis of novel phosphoramide-tegafur derivatives containing aminopropylsilatrane
DQ Shi, Q Chen, ZH Li, XP Liu
Index: De, Qing Shi; Chen, Qi; Zhong, Hua Li; Xiao, Peng Liu Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 7 p. 1621 - 1627
Abstract A series of novel phosphoramide-tegafur derivatives containing γ-aminopropyl silatrane were synthesized via the condensation reactions of phosphoryl dichloride with N1- (2-furanidyl)-N3-(hydroxyethyl)-5-fluorouracil, followed by condensation with γ-aminopropyl silatrane. The structures of the products were confirmed by 1H NMR, 31P NMR, IR, MS, and elemental analysis. The results of preliminary bioassay showed that the new compounds ...